Annual Reports on NMR Spectroscopy

Contributors

Preface

Chapter One. NMR Studies of Crown Ether–Cyclodextrin Complexes

Abstract

1 Introduction

2 Cyclodextrins: The Molecular Containers

3 Crown Ethers and Cryptands: The Beginning of Supramolecular Chemistry

4 Cyclodextrin–Crown Ether Complexes: Non-NMR Studies

5 Cyclodextrin–Crown Ether Interactions: An NMR Look

6 Complexes of Cyclam Derivatives

7 Conclusions

References

Chapter Two. ¹⁵N and ³¹P NMR Coordination Shifts in Transition Metal Complexes with Nitrogen- and Phosphorus-Containing Heterocycles

Abstract

1 Transition Metal Complexes with Azines

2 Transition Metal Complexes with Azoles

3 Transition Metal Complexes with Purines

4 Transition Metal Complexes with 1,2,4-Triazolo-[1,5a]-Pyrimidines

5 Transition Metal Complexes with Phosphinines

6 Transition Metal Complexes with Phospholes

7 Conclusions

References

Chapter Three. Quantification of Complex Mixtures by NMR

Abstract

1 Introduction

2 Practical Background

3 NMR Acquisition Methods

4 Post-Acquisition NMR Processing

5 Application Areas of qNMR

6 Future Developments

Acknowledgements

References

Chapter Four. Proton NMR Profiling of Food Samples

Abstract

1 Introduction

2 Sample Preparation

3 NMR Techniques

4 Data Treatment

5 Statistical Analysis

6 Applications

References

Chapter Five. Magic Angle Spinning NMR Studies of Protein Assemblies: Recent Advances in Methodology and Applications

Abstract

1 Introduction

2 Recent Methodological Advances for MAS NMR Studies of Protein Assemblies

3 Recent MAS NMR Applications to Study Protein Assemblies

4 Conclusions and Outlook

References

Chapter Six. Recent Advances in Solution NMR Studies: ¹³C Direct Detection for Biomolecular NMR Applications

Abstract

1 Introduction

2 Intrinsic Properties of Heteronuclei (¹³C, ¹⁵N)

3 Examples of Applications

References

Index