Methods of Surface Analysis of Heterogeneous Catalysts

This two-volume work provides an overview of the most common spectroscopic techniques which have been applied to reveal catalyst structures and surface characteristics in both model catalysts and those of industrial importance. A great amount of work on catalyst characterization using spectroscopic probes has been undertaken from both fundamental and applied perspectives. However, this general information is in urgent need of a critical revision. To undertake this task, a number of experts in the fields of structural and surface characterization of heterogeneous catalysts have contributed to this book. Part A provides an up-to-date review of the theoretical basis and applications of spectroscopic methods to identify catalyst structures (photoelectron spectroscopy, ion scattering, infrared, extended X-ray absorption fine structure, Mössbauer). Part B concentrates on catalyst surfaces. The interaction of adsorbed molecules, mostly on heterogenous catalysts, although some reference to model catalysts is also made, is discussed here. Vibrational (infrared and electron energy loss spectroscopies, magnetic resonances (nuclear and electron spin) and thermal desorption methods have been included in this latter category. The reader will find also a comparison of these well established methods with their recent developments which make them much more attractive. Therefore, researchers working in the catalysis field will find much to interest them in this book.